Aminoacetonitrile hydrochloride
Glycinonitrile hydrochloride
CAS: 6011-14-9
Molecular Formula: C2H5ClN2
Aminoacetonitrile hydrochloride - Names and Identifiers
Aminoacetonitrile hydrochloride - Physico-chemical Properties
| Molecular Formula | C2H5ClN2 |
| Molar Mass | 92.53 |
| Melting Point | 172-174°C |
| Boling Point | 164.2°C at 760 mmHg |
| Flash Point | 53.1°C |
| Water Solubility | Soluble in water 20°C, 1000g/L. |
| Solubility | Methanol (Slightly, Heated), Water |
| Vapor Presure | 1.99mmHg at 25°C |
| Appearance | White solid |
| Color | White to Off-White |
| Merck | 14,412 |
| Storage Condition | Inert atmosphere,Room Temperature |
| Sensitive | Hygroscopic |
| MDL | MFCD00012850 |
| Physical and Chemical Properties | Melting Point: 172 - 174 character: hygroscopic |
| Use | Used as pharmaceutical intermediates, raw materials for organic synthesis |
Aminoacetonitrile hydrochloride - Risk and Safety
| Risk Codes | R20/21/22 - Harmful by inhalation, in contact with skin and if swallowed. R36/37/38 - Irritating to eyes, respiratory system and skin. R25 - Toxic if swallowed |
| Safety Description | S22 - Do not breathe dust. S36/37 - Wear suitable protective clothing and gloves. S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. |
| UN IDs | 3439 |
| RTECS | MC1950000 |
| TSCA | Yes |
| HS Code | 29269090 |
| Hazard Class | 6.1 |
| Packing Group | III |
Aminoacetonitrile hydrochloride - Reference Information
| EPA chemical substance information | information provided by: ofmpeb.epa.gov (external link) |
| synthesis method | (1), ammonia chloride, Formaldehyde, Acetic acid and sodium cyanide as reaction raw materials, the condensation reaction generates amino acetonitrile: first, 53.5g of ammonia chloride, 37% g of formaldehyde 162g and 267.5g of water are added to the reactor, stirred evenly, and then cooled to below 0 °c, then 40% g of 122.5 sodium cyanide aqueous solution was added dropwise, Dropwise added to half, and 42g of acetic acid was added dropwise at the same time, then the reaction was continued for 1-2 hours below 0 ℃, and then filtered, 48g of aminoacetonitrile was obtained by centrifugation. (2) reacting aminoacetonitrile with a methanol solution of hydrogen chloride to produce aminoethylenitrile hydrochloride: 48g of aminoacetonitrile and 90g of a methanol solution of hydrogen chloride obtained in step (1) (the content of hydrochloric acid in the solution is 30%, control the moisture content below 1%) mixed, reacted at 45-50 ℃ for 1-2 hours, then cooled to below 5 ℃, filtered, centrifuged, and baked to obtain 58.3g of aminoacetonamide hydrochloride, the total molar yield was calculated to be 63.03%. |
| Use | used as pharmaceutical intermediates, organic synthesis raw materials |
Last Update：2024-04-09 02:00:09
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